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Analytical Pyrolysis Handbook
by Karen D. SamAnalytical pyrolysis allows scientists to use routine laboratory instrumentation for analyzing complex, opaque, or insoluble samples more effectively than other analytical techniques alone. Analytical Pyrolysis Handbook, Third Edition is a practical guide to the application of pyrolysis techniques to various samples and sample types for a diversity of fields including microbiology, forensic science, industrial research, and environmental analysis. The much-anticipated third edition incorporates recent technological advances that increase the technique’s sensitivity to trace elements, improve its reproducibility, and expand its applicability. The book reviews the types of instrumentation available to perform pyrolysis and offers guidance for interfacing instruments and integrating other analytical techniques, including gas chromatography and mass spectrometry. Fully updated with new sample pyrograms, figures, references, and real-world examples, this edition also highlights new areas of application including cultural materials, forensic analysis, and environmental studies. This book illustrates how the latest advances make pyrolysis a practical, cost-effective, reliable, and flexible alternative for increasingly complex sample analyses. Analytical Pyrolysis Handbook, Third Edition is an essential, one-stop guide for determining if pyrolysis meets application-specific needs as well as performing pyrolysis and handling the data obtained.
Analytical Scientists in Pharmaceutical Product Development: Task Management and Practical Knowledge
by Kangping XiaoThis book explains task management concepts and outlines practical knowledge to help pharmaceutical analytical scientists become productive and enhance their career. •Presents broad topics such as product development process, regulatory requirement, task and project management, innovation mindset, molecular recognition, separation science, degradation chemistry, and statistics. •Provokes thinking through figures, tables, and case studies to help understand how the various functions integrate and how analytical development can work efficiently and effectively by applying science and creativity in their work. •Discusses how to efficiently develop a fit-for-purpose HPLC method without screening dozens of columns, gradients, or mobile phase combinations each time, since the extra effort may not provide enough of a benefit to justify the cost and time in a fast-paced product development environment. This book explains task management concepts and outlines practical knowledge to help pharmaceutical analytical scientists become productive and enhance their career. •Presents broad topics such as product development process, regulatory requirement, task and project management, innovation mindset, molecular recognition, separation science, degradation chemistry, and statistics. •Provokes thinking through figures, tables, and case studies to help understand how the various functions integrate and how analytical development can work efficiently and effectively by applying science and creativity in their work. •Discusses how to efficiently develop a fit-for-purpose HPLC method without screening dozens of columns, gradients, or mobile phase combinations each time, since the extra effort may not provide enough of a benefit to justify the cost and time in a fast-paced product development environment.
Analytical Skills for AI and Data Science: Building Skills for an AI-Driven Enterprise
by Daniel VaughanWhile several market-leading companies have successfully transformed their business models by following data- and AI-driven paths, the vast majority have yet to reap the benefits. How can your business and analytics units gain a competitive advantage by capturing the full potential of this predictive revolution? This practical guide presents a battle-tested end-to-end method to help you translate business decisions into tractable prescriptive solutions using data and AI as fundamental inputs.Author Daniel Vaughan shows data scientists, analytics practitioners, and others interested in using AI to transform their businesses not only how to ask the right questions but also how to generate value using modern AI technologies and decision-making principles. You’ll explore several use cases common to many enterprises, complete with examples you can apply when working to solve your own issues.Break business decisions into stages that can be tackled using different skills from the analytical toolboxIdentify and embrace uncertainty in decision making and protect against common human biasesCustomize optimal decisions to different customers using predictive and prescriptive methods and technologiesAsk business questions that create high value through AI- and data-driven technologies
Analytical Solutions for Transport Processes: Fluid Mechanics, Heat and Mass Transfer (Mathematical Engineering)
by Günter BrennThis monograph provides analytical solutions to a number of classical problems in transport processes, i. e. in fluid mechanics, heat and mass transfer. Increasing computing power and efficient numerical methods have increased the importance of computational tools. However, the interpretation of these results is often difficult and the computational results need to be tested against the analytical results. This is why the analytical solutions are of high value. Furthermore, analytical solutions for transport processes provide a much deeper understanding of the physical phenomena of a given process than the corresponding numerical solution. The target audience primarily comprises researcher and practitioners but the book may also be beneficial for graduate students who want to enter the field.
Analytical Techniques for Biopharmaceutical Development
by Stephen Tuck Tim Wehr Roberto Rodriquez-DiazThis reference assists scientists in the selection and application of analytical techniques for biopharmaceutical identification, formulation, and assessment-providing a valuable survey of exploratory methods commonly utilized during the preclinical, clinical, and commercial phases of development.
Analytical Techniques for Clinical Chemistry
by Sergio Caroli Gyula ZárayDiscover how analytical chemistry supports the latest clinical research This book details the role played by analytical chemistry in fostering clinical research. Readers will discover how a broad range of analytical techniques support all phases of clinical research, from early stages to the implementation of practical applications. Moreover, the contributing authors' careful step-by-step guidance enables readers to better understand standardized techniques and steer clear of everyday problems that can arise in the lab. Analytical Techniques for Clinical Chemistry opens with an overview of the legal and regulatory framework governing clinical lab analysis. Next, it details the latest progress in instrumentation and applications in such fields as biomonitoring, diagnostics, food quality, biomarkers, pharmaceuticals, and forensics. Comprised of twenty-five chapters divided into three sections exploring Fundamentals, Selected Applications, and Future Trends, the book covers such critical topics as: Uncertainty in clinical chemistry measurements Metal toxicology in clinical, forensic, and chemical pathology Role of analytical chemistry in the safety of drug therapy Atomic spectrometric techniques for the analysis of clinical samples Biosensors for drug analysis Use of X-ray techniques in medical research Each chapter is written by one or more leading pioneers and experts in analytical chemistry. Contributions are based on a thorough review and analysis of the current literature as well as the authors' own firsthand experiences in the lab. References at the end of each chapter serve as a gateway to the literature, enabling readers to explore individual topics in greater depth. Presenting the latest achievements and challenges in the field, Analytical Techniques for Clinical Chemistry sets the foundation for future advances in laboratory research techniques.
Analytical Techniques for Natural Product Research
by Satyanshu KumarPlants are important source of lead molecules for drug discovery. These lead molecules serve as starting materials for laboratory synthesis of drug as well a model for production of biologically active compounds. Phytochemical processing of raw plant materials is essentially required to optimize the concentration of known constituents and also to maintain their activities. Extraction techniques and analytical techniques have played critical roles in phytochemical processing of raw materials. Extraction technologies from conventional extraction to green extraction as well as analytical techniques from single technique to hyphenated/coupled techniques most frequently used in phytochemistry laboratories are covered in the book.
Analytical Techniques for Natural Product Research
by Satyanshu KumarPlants are important source of lead molecules for drug discovery. These lead molecules serve as starting materials for laboratory synthesis of drug as well a model for production of biologically active compounds. Phytochemical processing of raw plant materials is essentially required to optimize the concentration of known constituents and also to maintain their activities. Extraction techniques and analytical techniques have played critical roles in phytochemical processing of raw materials. Extraction technologies from conventional extraction to green extraction as well as analytical techniques from single technique to hyphenated/coupled techniques most frequently used in phytochemistry laboratories are covered in the book.
Analytical Techniques for Studying the Physical Properties of Lipid Emulsions (SpringerBriefs in Food, Health, and Nutrition #3)
by Maria Lidia HerreraThis book will review old and new methods to study emulsion stability and structure. Examples of emulsion-based foods include ice cream, yoghurt, and mayonnaise. The physicochemical properties of emulsions play an important role in food systems, as they directly contribute to the texture, sensory and nutritional properties of foods. One of the main properties is stability, which refers to the ability of an emulsion to resist physical changes over time. The development of an effective strategy to prevent undesirable changes in the properties of a particular food emulsion depends on the dominant physicochemical mechanism(s) responsible for the changes. In practice, two or more of these mechanisms may operate in concert. It is therefore important for food scientists to identify the relative importance of each mechanism, the relationship between them, and the factors that influence them, so that effective means of controlling the stability and physicochemical properties of emulsions can be established. Several techniques are used to study the physical behavior and structure of emulsions. Each technique has its advantages and disadvantages and provides different insights into the destabilization mechanisms. Among the oldest methods used to study emulsion stability is visual observation and small deformation rheometry. More recently, other techniques, such as ultrasound profiling, microscopy, droplet size distribution, and measurement of surface concentration to characterize adsorbed protein at the interface, have also been employed. Some of these techniques, such as droplet size distribution, involve some form of dilution. However, dilution disrupts some structures that play an important role in stability. The ability to study the stability of food emulsions in their undiluted form may reveal subtle nuances about their stability. Diffusing wave spectroscopy (DWS), laser scanning confocal microscopy (LSCM), nuclear magnetic resonance (NMR), and Turbiscan are among the more powerful, non-perturbing techniques used to characterized emulsions.
Analytical Techniques for the Elucidation of Protein Function
by Isao Suetake Rohit K. Sharma Hironobu HojoANALYTICAL TECHNIQUES FOR THE ELUCIDATION OF PROTEIN FUNCTION An essential aid for scientists seeking alternative techniques for investigating proteins Proteins are the building blocks of living organisms, and they play an enormous range of fundamental roles in sustaining and shaping life. The critical determinant of a protein’s function is its structure, and the analysis of protein structures has therefore become a significant component of biological research. In recent years, longstanding analytical techniques such as X-ray crystallography and nuclear magnetic resonance (NMR) spectroscopy have been supplemented by a number of new methods which promise to revolutionize the study of proteins and their functions. Analytical Techniques for the Elucidation of Protein Function serves as an introduction to these techniques, which are especially crucial for analyzing intrinsically disordered regions and post-translational modifications. These have revolutionized the study of proteins in recent years, and conventional methods for analyzing protein structures are no longer sufficient to work through their ramifications. This book therefore brings greater awareness of techniques which promise to produce the very cutting edge of protein research. Analytical Techniques for the Elucidation of Protein Function readers will find: A discussion of techniques including electron paramagnetic resonance (ESR) spectroscopy, neutron scattering, Raman imaging, and more Both theoretical background and practical applications for each technique Contributions from leading international researchers into protein structure and function This practically focused text is a valuable reference for protein and peptide analysis and synthesis researchers, as well as for graduate and advanced undergraduate students in the life sciences.
Analytical Techniques in Biochemistry (Springer Protocols Handbooks)
by Mahin BashaThis book provides a comprehensive overview of the major biochemical analytical techniques, with detailed descriptions of the instrumentation and applications. The contributions, which each focus on a specific technique, are based on a thorough review and analysis of the current literature as well as the authors’ experiences in the lab. Divided into nine parts, the book provides insights into basic separation techniques like sedimentation, filtration and centrifugation, as well as analytical techniques such as spectrophotometry, chromatography, electrophoresis, immuno-techniques, radioactivity and microscopy.
Analytical Techniques in Biochemistry and Molecular Biology
by Rajan KatochAdvances in biochemistry now allow us to control living systems in ways that were undreamt of a decade ago. This volume guides researchers and students through the full spectrum of experimental protocols used in biochemistry, plant biology and biotechnology.
Analytical Techniques in Forensic Science
by Rosalind WolstenholmeAn in-depth text that explores the interface between analytical chemistry and trace evidence Analytical Techniques in Forensic Science is a comprehensive guide written in accessible terms that examines the interface between analytical chemistry and trace evidence in forensic science. With contributions from noted experts on the topic, the text features a detailed introduction analysis in forensic science and then subsequent chapters explore the laboratory techniques grouped by shared operating principles. For each technique, the authors incorporate specific theory, application to forensic analytics, interpretation, forensic specific developments, and illustrative case studies. Forensic techniques covered include UV-Vis and vibrational spectroscopy, mass spectrometry and gas and liquid chromatography. The applications reviewed include evidence types such as fibers, paint, drugs and explosives. The authors highlight data collection, subsequent analysis, what information has been obtained and what this means in the context of a case. The text shows how analytical chemistry and trace evidence can problem solve the nature of much of forensic analysis. This important text: Puts the focus on trace evidence and analytical science Contains case studies that illustrate theory in practice Includes contributions from experts on the topics of instrumentation, theory, and case examples Explores novel and future applications for analytical techniques Written for undergraduate and graduate students in forensic chemistry and forensic practitioners and researchers, Analytical Techniques in Forensic Science offers a text that bridges the gap between introductory textbooks and professional level literature.
Analytical Techniques in the Oil and Gas Industry for Environmental Monitoring
by Melissa N. Dunkle William L. WinnifordA thorough introduction to environmental monitoring in the oil and gas industry Analytical Techniques in the Oil and Gas Industry for Environmental Monitoring examines the analytical side of the oil and gas industry as it also provides an overall introduction to the industry. You’ll discover how oil and natural gas are sourced, refined, and processed. You can learn about what’s produced from oil and natural gas, and why evaluating these sourced resources is important. The book discusses the conventional analyses for oil and natural gas feeds, along with their limitations. It offers detailed descriptions of advanced analytical techniques that are commercially available, plus explanations of gas and oil industry equipment and instrumentation. You’ll find technique descriptions supplemented with a list of references as well as with real-life application examples. With this book as a reference, you can prepare to apply specific analytical methods in your organization’s lab environment. Analytical Techniques can also serve as your comprehensive resource on key techniques in the characterization of oil and gas samples, within both refinery and environmental contexts. Understand of the scope of oil and gas industry techniques available Consider the benefits and limitations of each available process Prepare for applying analytical techniques in your lab See real examples and a list of references for each technique Read descriptions of off-line analytics, as well as on-line and process applications As a chemist, engineer, instructor, or student, this book will also expand your awareness of the role these techniques have in environmental monitoring and environmental impact assessments.
Analytical Testing for the Pharmaceutical GMP Laboratory
by Kim Huynh-BaProvides practical guidance on pharmaceutical analysis, written by leading experts with extensive industry experience Analytical Testing for the Pharmaceutical GMP Laboratory presents a thorough overview of the pharmaceutical regulations, working processes, and drug development best practices used to maintain the quality and integrity of medicines. With a focus on smaller molecular weight drug substances and products, the book provides the knowledge necessary for establishing the pharmaceutical laboratory to support Quality Systems while maintaining compliance with Good Manufacturing Practices (GMP) regulations. Concise yet comprehensive chapters contain up-to-date coverage of drug regulations, pharmaceutical analysis methodologies, control strategies, testing development and validation, method transfer, electronic data documentation, and more. Each chapter includes a table of contents, definitions of acronyms, a reference list, and ample tables and figures. Addressing the principal activities and regulatory challenges of analytical testing in the development and manufacturing of pharmaceutical drug products, this authoritative resource: Describes the structure, roles, core guidelines, and GMP regulations of the FDA and ICH. Covers the common analytical technologies used in pharmaceutical laboratories, including examples of analytical techniques used for the release and stability testing of drugs. Examines control strategies established from quality systems supported by real-world case studies. Explains the use of dissolution testing for products such as extended-release capsules, aerosols, and inhalers. Discusses good documentation and data reporting practices, stability programs, and the Laboratory Information Management System (LIMS) to maintain compliance. Includes calculations, application examples, and illustrations to assist readers in day-to-day laboratory operations. Contains practical information and templates to structure internal processes or common Standard Operating Procedures (SOPs). Analytical Testing for the Pharmaceutical GMP Laboratory is a must-have reference for both early-career and experienced pharmaceutical scientists, analytical chemists, pharmacists, and quality control professionals. It is also both a resource for GMP laboratory training programs and an excellent textbook for undergraduate and graduate courses of analytical chemistry in pharmaceutical sciences or regulatory compliance programs.
Analytical Thermodynamics
by Dongqing LiThis book provides the foundations of analytical thermodynamics for graduate level. The content is based on the author’s lecture notes developed over 30 years of academic teaching. It aims to present thermodynamics to the readers as easy to understand as possible, being suitable for professors teaching advanced thermodynamics or graduate students learning thermodynamics. The chapters include the basics of analytical thermodynamics, modelling of homogeneous and heterogeneous systems, thermodynamics of interfaces and three-phase contact lines and the Second Law in engineering thermodynamics.
Analytical Thermodynamics
by Dongqing LiThis second edition presents an enriched and expanded exploration of the fundamental principles of thermodynamics tailored for graduate-level studies. Drawing on over three decades of academic teaching experience, the author has refined the content, making it more accessible and comprehensive. Chapter 1 has been restructured for clarity, delineating "Legendre Transformation" and "Thermodynamic Potentials" into separate sections, while the treatment of "Chemical Potentials" has been significantly augmented, encompassing two-component ideal gas mixtures and a re-derivation of chemical potentials for dilute solutions. Additionally, the section on thermodynamic stability now boasts enhanced explanations and illustrative figures. Chapter 2 introduces a groundbreaking section, "Electrolyte Solution in Electric Field as a Non-Uniform System," providing fresh insights into unexplored realms. Chapter 3, now enriched with several new sections, delves into topics such as "Contact Angles on Heterogeneous Surfaces and Rough Surfaces," "Elastic Liquid-Fluid Interface," "Curvature Effect on Surface Tension," "Solute Effect on Equilibrium Pressure," and "Heterogeneous Bubble Nucleation in a Dilute Solution." Chapter 4 features new elucidations and discussions aimed at bolstering comprehension, while the entirely new Chapter 5 offers solutions to selected homework and exam questions, adding a practical dimension to the theoretical framework. This edition, encompassing approximately 50% new content, expands the book by 131 pages, rendering it an even more invaluable resource for professors instructing advanced thermodynamics and graduate students delving into this intricate subject matter.
Analytical Tools for Assessing the Chemical Safety of Meat and Poultry (SpringerBriefs in Food, Health, and Nutrition #9)
by Fidel Toldrá Milagro ReigThe goal of the Brief is to summarize the state of the art on the chemical safety issues currently concerning meat and poultry, and to discuss the current international legislation on the tools available for their control. The Brief will review the analytical controls and instrumentation available for the control of residues of growth promoters, antibiotics, and any other environmental substances in raw meat and poultry. In addition, there will be a discussion of both the substances that may be generated as a consequence of processing, and the tools that are available for their control. These substances may be quite varied in nature; they may include, for example, the heterocyclic amines generated by heating, the nitrosamines sometimes present in cured meats with nitrite if not properly processed, the polycyclic aromatic hydrocarbons that can be generated depending on the type of smoking used, or the biogenic amines that can be generated during fermentation. Finally, the controls for the detection of foreign proteins (e.g., whey proteins) in the final products will be also compiled. The Brief will conclude with a view of future trends and key references for readers interested in learning more about this topic.
Analytical Transmission Electron Microscopy: An Introduction for Operators
by Jürgen Thomas Thomas GemmingThis work is based on experiences acquired by the authors regarding often asked questions and problems during manifold education of beginners in analytical transmission electron microscopy. These experiences are summarised illustratively in this textbook. Explanations based on simple models and hints for the practical work are the focal points. This practically- oriented textbook represents a clear and comprehensible introduction for all persons who want to use a transmission electron microscope in practice but who are not specially qualified electron microscopists up to now.
Analytical and Approximate Methods for Complex Dynamical Systems (Understanding Complex Systems)
by Alexander TimokhaThis book presents Analytical and Approximate Methods for Complex Dynamical Systems and introduces ideas of discontinuous mapping treated as complex dynamical systems. Mathematicians of world-recognized Ukrainian scientific schools established by M.Krylov, M.Bogolyubov, Yu.Mitropolskiy, and A.Sharkovsky used to cooperate for writing the collective book whose purpose consists of illustrating a synergy of combining diverse (by idea and technique) constructive analytical and approximate approaches and methods in complex dynamical systems which are herein associated with mathematical models of networks, conflict/economic theories, sloshing, soft matter, and even levitating drops. Readers are facilitated to learn contemporary insights, fundamentals (Parts I and III), applications (Part II), and components of theories of bifurcation, synchronization/self-organization, collective dynamics, chaos, solitons, fractional differential equations, symmetry, reduced order modelling, and many others, that makes the book useful for both graduate and postgraduate students, lecturers, researchers, and even engineers dealing with multidimensional dynamic systems.
Analytical and Approximate Methods in Transport Phenomena
by Marcio L. de Souza-SantosOn the job or in the field, when facing a problem with differential equations and boundary conditions, most likely you don't have time to read through several publications in search of a method that may or may not solve your problem. Organized for quick and easy access to practical solutions, Analytical and Approximate Methods in Transport Pheno
Analytical and Experimental Modal Analysis
by Subodh V. ModakThis book covers the fundamentals and basic concepts of analytical and experimental approaches to modal analysis. In practice, the analytical approach based on lumped parameter and finite element models is widely used for modal analysis and simulation, and experimental modal analysis is widely used for modal identification and model validation. This book is inspired by this consideration and is written to give a complete picture of modal analysis. Features: Presents a systematic development of the relevant concepts and methods of the analytical and experimental modal analyses. Covers phase resonance testing and operational modal analysis. Provides the relevant signal processing concepts. Includes applications like model validation and updating, force identification and structural modification. Contains simulations, examples, and MATLAB® programs to enhance understanding. This book is aimed at senior undergraduates/graduates, researchers, and engineers from mechanical, aerospace, automotive, civil, and structural engineering disciplines.
Analytical and Practical Aspects of Drug Testing in Hair (International Forensic Science and Investigation)
by Pascal KintzWritten by well-known, international authors, this comprehensive reference provides practical coverage of the best hair drug testing techniques and examines the drugs themselves. The authors review all new developments, the validation of analytical procedures, and the interpretation of data. Some of the applications discussed include doping, drug-facilitated crime investigating, workplace testing, and the granting of drivers' licenses. The authors describe specific drugs, such as opiates, cocaine, and cannabis, and discuss the different testing methods of them. The book also covers postmortem toxicology, pitfalls created by passive exposure, and testing for metals, including inductively coupled plasma spectrometry (ICP-MS), hair multielemen
Analytical and Preparative Separation Methods of Biomacromolecules
by Hassan Y. Aboul-EneinReports up-to-date research developments on purifying and isolation large organic molecules. The text provides information on high-performance liquid chromatography and capillary electrophoresis (CE) as tools for analyzing biomacromolecules and developing new biochemical and medicinal compounds. It applies biochemical separation technology to the study of macromolecules such as proteins, polysaccharides, nucleic acids and more.
Analytical or Semi-analytical Solutions of Functionally Graded Material Structures
by Zheng Zhong Guojun NieThis book provides a comprehensive introduction to the analysis of functionally graded materials and structures. Functionally graded materials (FGMs), in which the volume fractions of two or more constituent materials are designed to vary continuously as a function of position along certain direction(s), have been developed and studied over the past three decades. The major advantage of FGMs is that no distinct internal boundaries exist, and failures from interfacial stress concentrations developed in conventional components can be avoided. The gradual change of material properties can be tailored to different applications and working environments. As these materials’ range of application expands, new methodologies have to be developed to characterize them, and to design and analyze structural components made of them.Despite a number of existing papers on the analysis of functionally graded materials and structures, there is no single book that is devoted entirely to the analysis of functionally graded beams, plates and shells using different methods, e.g.,analytical or semi-analytical methods.Filling this gap in the literature, the book offers a valuable reference resource for senior undergraduates, graduate students, researchers, and engineers in this field. The results presented here can be used as a benchmark for checking the validity and accuracy of other numerical solutions. They can also be used directly in the design of functionally graded materials and structures.